Silibase is one of the leading & professional manufacturers specialized in producing all kinds of SILICONE BASED new materials.
Silibase technique team always focus on quality first and insist on developing new products.
Silibase people will serve you the best before and after sale.
Dec 19, 2017
Silane coupling agent process flow Briefing: A certain amount of purified trichlorosilane (98%) and allyl chloride (99%) first into the mixing kettle and thoroughly mixed under nitrogen atmosphere with the bulk of the platinum compound Isopropanol solution into a vacuum of 0.03-0.04Mpa and flush with nitrogen addition kettle, oil bath heating, the control temperature at 50 ~ 60 ℃, fully reacted for 5 to 6 hours, during the reaction catalyst After the batch is added, the reaction solution is gradually warmed to 80 ° C. and refluxed. When the reflux solution gradually decreases until the reflux solution can not be seen, the reaction is terminated and the reaction solution is sent to a fractionator for fractionation. The pressure in the autoclave 0.04Mpa, temperature control at 160 ℃, points to low boiling point, the crude product was further distilled to obtain γ-chloropropyl trichlorosilane products.